《Method C-02.2微波消解法测定表面涂层中的铅含量》.pdf

Product Safety Laboratory Book 5 - Laboratory Policies and Procedures 1 of 8 2007-06-08 Part B: Test Methods Section, Method C-02.2 Determination of Total Lead in Surface Coating Materials by Closed Vessel Microwave Digestion 45 1 SCOPE 1.1 This method describes a general procedure for the determination of the total lead content in surface coating materials as applicable to items 2, 9 and 18 of Part I, and item 31 of Part II of Schedule I to the Hazardous Products Act and the Surface Coating Materials Regulation (SOR 2005). 2 APPLICABLE DOCUMENTS 2.1 CGSB 1-GP-500.1, Methods of Test for Toxic Trace Elements in Protective Coatings - Determination of Lead (Pb) in Low Concentration. 2.2 Health Canada, Product Safety Bureau, SLSD Test Method C-02, Determination of Total Lead in Paints and Applied Coatings. 2.3 C. Watson, “The Determination of the Limit of Detection and the Limit of Quantification for the Varian Atomic Absorption Spectrometer” (SpectrAA220FS) Following Method C02.2, “Determination of Total Lead in Paints and Applied Coatings by Closed Vessel Microwave Digestion.” Health Canada, Product Safety Laboratory, Project report no 2001-0637. 2.4 A. Soucy, N. Ritchot, C. Watson, “Evaluation and Validation of Performance of the New Varian Atomic Absorption Spectrometer (AAS) Used for the Determination of Total Lead in Consumer Products.” Health Canada, Product Safety Laboratory, Project report no. 2001-0616. 2.5 B. Séguin, M. Charette, C. Watson, A. Soucy, “Development of an