ICP_AES法测定氧化铁粉中的硅_铝_钙_锰和硫_闻向东.pdfVIP

2008 8 A ug ust 200 8 36 4 Research on Iron St eel V ol. 36 No. 4 # 4 5 # ICP-AES 闻向东, 曹宏燕, 杨 芸 ( ( ) , 430080) : ICP- A ES , , F e O , r 0 . 999 9 2 3 0 . 000 4 % ~ 0. 001 % , 0 . 004 % , : ICP- A ES; ; ; ; ; ; : O567 . 31 : A : 1001- 1447 ( 2008) 04- 004 5- 0 3 Determination of oxides of silicon, aluminium, calcium, manganese and sulphur in iron oxide powder by ICP-AES WEN X ang- dong , CA O H ong- yan, Y A N G Y un ( Research and Development Cent er of WISCO, Wuhan 4 30080, Ch na) Abstract: T h s paper st ud es t he t est cond t ons of ICP- A ES method that s u sed t o de- t er m ne the content of ox des o f s l con , alum n um, calc um, manganese and sulphur n ron o x de pow der . When sam ples w ere d ssolv ed w t h co ncent rat ed hy dro chlor c ac d, t he so lut on rate w as h gher and the blank value of t est w as low er . T he cal brat o n g raphs w ere prepared u s ng st andard solut on conta n ng pur t y ro n ox de, t he cor rela- t on co ef f c ent ( r ) w as 0 . 999 9 . T he detect on l m t w as n a range of 0. 000 4 % ~ 0. 001 % f or S O2 , A l2 O3 , CaO , M nO , and 0. 004 % f or SO4 2- . T he m et hod has been successfully u sed t o det erm ne t he t race cont ent of ox des of s l co n, alum n um, calc- um , sulphur and mang anese n ro n ox de po w der w t h h gh accuracy and prec