溶胶-凝胶自蔓燃法制备Al2ZrO5纳米颗粒增强铝基复合材料.pdfVIP

Trans. Nonferrous Met. Soc. China 23(2013) 1556−1562 Fabrication of aluminum matrix composites reinforced with Al ZrO nano particulates synthesized by sol−gel auto-combustion method 2 5 S. A. KHORRAMIE1 2 3 , M. A. BAGHCHESARA , D. P. GOHARI 1. Department of Chemistry, North Tehran Branch, Islamic Azad University, Tehran 14358-84381, Iran; 2. Department of Metallurgy Materials Engineering, Masjed Soleiman Branch, Islamic Azad University, Masjed Soleiman 64915-111, Iran; 3. Young Researchers and Elite Club, South Tehran Branch, Islamic Azad University, Tehran 14358-84381, Iran Received 20 July 2012; accepted 29 November 2012 Abstract: Nanocrystalline Al ZrO with particle size of about 38 nm was directly synthesized by combination of sol−gel 2 5 auto-combustion and ultrasonic irradiation techniques from metal nitrates and glycine as precursors. The overall process involves formation of homogeneous sol, formation of dried gel and combustion process of the dried gel. Aluminum alloy matrix composites reinforced with 0.75%, 1.5% and 2.5% Al2ZrO5 nanoparticles were fabricated via stir casting method and the fabrication was performed at various casting temperatures. The resulting composites were tested for their nanostructure and present phases by SEM and XRD analysis. Optimum amount of reinforcement and casting temperature were determined by evaluating the density, hardness and compression strength of the composites. Al matrix alloy reinforced by Al2ZrO5 nanopar