ecnultraeuenvironmentandclimatecontractnoenv4-ct97-0568（13页）.docVIP

RP – DRAFT - ELEMENTAL ANALYSIS OF AMBIENT AIR PARTICUALATE SAMPLES COLLECTED FROM SEAS USING GFAAS-Z Identification code: RP GFAAS-Z APPROVALS RP Working RP pages Issue Date: 01/04/2001 Local PI:01/22/2001 Revision No:1 Revision date:06/10/2002 Revision description: End cap GF tubes and 5% H2 for group 2 elements. Improved detection limits for As, Se, Pb and Ni Local PI: Revision No:3 Revision date:5/1/03 Revision description: Inclusion of NIST’s interim PM2.5 RM results for method validation. Local PI: Revision No: Revision date: / . Revision description: Local PI: Distributed to: Name of recipient: Original date Rev. 1. date Rev. 2. date Rev. 3. date Dr Phil Hopke 1/4/01 1/9/01 Dr John Ondov ELEMENTAL ANALYSIS OF AMBIENT AIR PARTICUALATE SAMPLES COLLECTED FROM SEAS USING GFAAS-Z 1. PURPOSE AND APPLICABILITY This research protocol (RP) contains protocol for performing multi elemental analysis of aqueous slurry samples using Perkin-Elmer SIMAA 6000. This is an evaluation version of an anticipated standard operating procedure (SOP), which will result from experiences with this RP. Due to this fact, this RP is subject to change. The SIMAA6000 is capable of determining upto six elements simultaneously. Samples are analyzed for multiple multielement suites to achieve analyses for all of the elements desired. Note that the number and choice of elements to be determined in each analytical suite are being reoptimized, and both are subject to change. 2. REFERENCES The Perkin Elmer SIMAA 6000 Instrument Manual, ‘Installation, Maintenance, and System Description’ (Part Number 0993-5218). The Perkin Elmer SIMAA 6000 Instrument Manual, ‘Setting Up and Performing Analyses’ (Part Number 0993-5219). The Perkin Elmer SIMAA 6000 Instrument Manual,