钛阳极氧化作业指导书[精选].doc

导言INTRODUCTION： 该工作细则旨在解释说明如何进行钛阳极化操作。 The purpose of this work instruction is to illustrate how to perform the titanium anodize operation. 参考资料REFERENCES： 外部标准External Standards： ASTM F86 –外科金属植入物的表面预处理和打标实践 ASTM F86 – Practice for Surface Preparation and Marking of Metallic Surgical Implants 所需资源REQUIRED RESOURCES： Timer 计时器 Hydrofluoric Acid 氢氟酸 RO/DI Water 反渗透去离子水 Hot Plate 加热板 Thermometer 温度计 Non-Latex Gloves 非乳胶手套 Strainers 滤网 Phosphoric Acid 磷酸 Sodium Bicarbonate 碳酸氢钠 Tanks 水槽 Nitric Acid 硝酸 Graduated Cylinders/Beakers 量筒/烧杯 Titanium Mesh 钛网 Color Range Gauge 颜色规 Ultrasonic Cleaner 超声波清洗机 Sodium Carbonate 碳酸钠 Perforated Polypropylene Sheet 穿孔聚丙烯薄板 304 SST – Mesh or Plates 304SST- 网或者托盘 Power Supply 电源 Digital Scale 数字天平 流程PROCEDURE： 环节 A – 钛阳极氧化过程 SECTION A – Titanium Anodize Process 步骤 Step 说明 Comment 附加说明Additional Comment (安全/质量/视图/资源/等等) (Safety/Quality/Visual/Resource/etc.) 设定计时器 Set timer 为下面酸洗步骤将计时器设定为30s～60s。 Set timer to 30s～60s for prepare of acid clean. 酸洗 Acid clean 将部件放入滤网，然后放入含有以下混合物的酸杯并用热板加热到35-40℃： 酸杯混合物配方：47毫升氢氟酸（浓度40%） 800毫升硝酸（浓度69%）, 1013 毫升反渗透/去离子水 Place strainer with parts into acid pre-treat container, heated to 35 - 40oC using a hot plate, and start timer. Solution formula:47 mL Hydrofluoric Acid (HF, 40%)，800 mL Nitric Acid (HN03, 69%), and1013 mL RO/DI Water 清洗 Cleaning 将部件取出并放入含有至少4000毫升反渗透/去离子水的1号槽。让部件在槽中浸泡至少10秒钟。 Remove parts from acid pre-treat and place into Tub #1 containing at least 4000 mL of RO/DI water. Allow parts to sit in tub for a minimum of 10 seconds. 碳酸氢钠溶液清洗 Clean by sodium bicarbonate solution 将部件移至碳酸氢钠溶液的2号槽中，在槽中浸泡最少10秒。 碳酸氢钠溶液的配方如下：含有每4000毫升反渗透/去离子水的，里面至少含有1/8杯（约30ml）。 Move parts into tub #2 containing sodium bicarbonate solution. Allow parts to sit in tub for Min 10 s. Sodium bicarbonate solution formula: Per 4000 mL RO/DI Water with minimum 1/8 cup (约30ml) of sodium bicarbonate. 清洗 Cleaning 将部件取出并放入含有至少4000毫升反渗透/去离子水的3号槽。让部件在槽中浸泡至少10秒钟并放在水槽内准备阳极氧化。。 Move parts into Tub #3 c