巴旦杏仁油脂的超临界二氧化碳萃取工艺及其成分.docVIP

巴旦杏仁油脂的超临界二氧化碳萃取工艺及其成分 阿吉姑·阿布都热西提1、2，4 张君萍1 西尔艾力·吐尔逊4 阿吉艾克拜尔·艾萨*1 (1.省部共建新疆特有药用资源利用国家重点实验室培育基地 中国科学院新疆理化技术研究所，乌鲁木齐 830011; 2.喀什大学化学与环境科学学院，喀什 844006；3.新疆维吾尔自治区维吾尔医药研究所，乌鲁木齐830000；4.中国科学院大学,北京100049) 摘 要：研究巴旦杏仁油的超临界CO2萃取工艺，通过单因素实验和正交实验设计探讨了萃取压力、温度、CO2流量和萃取时间对巴旦杏仁油超临界CO萃取得率的影响。结果表明萃取压力35 MPa ，萃取温度40 ℃，二氧化碳流量6 L/min，萃取时间4为最优条件，在此条件下巴旦杏仁油萃取得率达到43.10%；采用气相色谱质谱GC-MS）联用技术对巴旦杏仁油脂肪酸组成进行分析，结果表明巴旦杏仁油不饱和脂肪酸含量高达%，以油酸（%）、亚油酸（13.%）为主，饱和脂肪酸以棕榈酸（6.%）为超临界CO2萃取TS224.4） 文献标识码：A 文章编号：1003-0174（2015）04-0020-01 Study on Extraction of Almond Seed Oil by Supercritical Carbon Dioxide and Composition Analysis AJIGU·Abudurexiti1,2 ZHANG Jun-ping1 XIRALI·Tursun3 HAJIAKBR·Aisa1 (1.State Key Laboratory Basis of Xinjiang Indigenous Medicinal Plants Resource Utilization, Xinjiang Technical Institute of Physics and Chemistry, Chinese Academy of Sciences，Urumqi 830011; 2. of Chemistry and Environmental Science, Kashgar University, Kashgar 844006; 3.Institute of Xinjiang Traditional Uyghur Medicine, Urumqi 830000;4.University of Chinese Academy of Sciences,Beijing100049,China) Abstract：Supercritical CO2 extraction was applied to extract seed oil of Almond. Single factor and orthogonal experiment was used to investigate the effect of pressure, temperature, extraction time and CO2 flow rate on the yield of oil. The results showed that the optimal operation conditions were pressure 35MPa, temperature 40℃、extraction time 4h and CO2 flow rate 6L/min, under such conditions, the yield of oil reached 43.10%. The contents and composition of fatty acids were tested by GC-MS, the results indicated that the fatty acids in the oil were composed of 9.20% unsaturated fatty acids, oleic acid(78.448%) and linoleic acid (13.723%) and palmitic acid (6.018%) were the main fatty acids. Key words：supercritical CO2 extractionAlmond seed oil, GC-MS, fatty acid 巴旦杏仁为巴旦杏的干燥成熟种子。巴旦杏(Amygdalus communis L.)，又称扁桃，是蔷薇科(Rosaceae)李亚科(Pmnoideae)扁桃属(Amygdalus)乔木，集中分布在中国西北和西南地区，尤以新疆天山以南的喀什、阿克苏、和田、库尔勒和阿图什等地种植的较多[1]。 巴旦杏果肉干涩