二甲醚分离装置中的精馏工段工艺设计.docVIP

摘 要本设计主要针对分离中的精馏工段进行工艺设计，分离二甲醚、甲醇和水三元体系。查阅相关资料充分了解二甲醚的性质用途及其现有的分离工艺结合实际情况工艺。 通过基础数据的查找、处理得到相应条件下的基础数据。精馏塔采用浮阀塔，本设计较为突出的特点有以下几点：（1）塔顶采用液氨冷凝用来准确控制回流比（2）塔板结构设计中精馏段采用单溢流，提馏段则采用双溢流。 塔底采用水蒸汽加热，以提供足够的热量。再通过计算得出理论板数为7.76块，塔效率为0.292，实际板数为27块，进料位置为提馏段向上第十六块，在浮阀塔主要工艺尺寸的设计计算中得出精馏段塔径为1.6m，提馏段塔径为2.1m。有效塔高15.5m。通过浮阀的流体力学验算，用AutoCAD绘制负荷性能图证明各指标数据均符合标准。以保证精馏过程的顺利进行并使效率尽可能的提高。关键词：二甲醚；甲醇；水；三元体系；分离 Abstract The design conducts process programming to separate ternary system of dimethyl, methanol and water mainly based on distillation processes in separation. understanding the nature, application and existing separation process of dimethyl through searching relevant information. proposing separation process with actual situation. Basic data of corresponding conditions was obtained by searching and handling basic data. the float valve tower was considered as the primary device of distillation operation, there are several points for the innovation characteristic of the design: (1) liquid ammonia condensate in the top of the tower, it Was used to control reflux ratio accurately. (2) the rectifying section utilizes single overflow and the stripping section utilizes double overflow in design of trays structure. Water vapor provide enough heat in tower bottom. Theoretical plate number of 7.76, tower efficiency of 0.292, The actual number of trays of 27, Feed location locates in sixteenth trays above the stripping section by calculation, Column diameter of the rectifying section of 1.6 meters, column diameter of the stripping section of 2.1 meters and effective tower height of 15.5 meters in the main process size design calculations of float valve tower. each index data are in line with standards In order to ensure the smooth progress of the rectification process and improve efficiency as much as possible by checking hydrodynamics of float valve tower which drawed load performance with Auto CAD. Keywords: DME ; Methanol ; Water ; Ternary system ; Separation 毕业论文（设计）