仪器测试.PDFVIP

仪器测试 • 仪器: Agilent 7890 w/ FID • 柱子型号: GsBP-5MS 30m x 0.25mm x 0.25um • 炉温: 80 °C (hold 0.5 min) to 160 °C at 30 °C/min, to 240 °C(hold 2min) at 15 °C /min to 320 °C(hold 1min) at 8 °C/min. • 载气: 氢气, 柱流量1.5ml/min • 进样口: Split, 275 ℃, split flow 60ml/min • 探测器: FID 325 ℃ • 进样量: EPA 8061 standard 1ul FID1 A, Front Signal (2015-01-19 10-52-52.D) pA 5 4