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液晶环氧树脂的合成与固化行为研究论文
Abstract
fortheir desirable
resins as thermosets
engineering many
Epoxy a托widelyapplied
contain unitsin
rigid-rodmesogenic
properties.Liquid-crystallineepoxyresins(LCERs)that
theirbackbonehavebeen studiedfordecades.
extensively
Twonovel etherof etherof
4A’-bisphenylol(DGEBP)anddiglycidyl
LCERs,diglycidyl
were
4,4'-bis(4-hydroxybenzoyloxy)-3,3’,5,5’-tetramethyl
basedontherecentliteratures.Their structure,thermal
synthesized spectroscopic properties,
were FT
and stmctrure IILNM&GC-MS,elememanalysis(EA),
phase investigatedby
differentialcalorimetry(DSC)andpolarizedlight
scanning
theratioof2.8l:97.19.The
of werefoundGC.MSwith
Twoenanti-isomersDGEBP by
wasobservedDSCand
and structureofDGBBHBTMBP
polymesomorphous by
monotropic
PLM.
Curebehaviorsandthermal of
properties
werestudiedand eachothermeans
diamine(BPDA)systemscompared by
DGEBP/biphenyl
the
both duringcuring
ofDSCandPLM.For appeared
systems,themesogemcphase
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