原子荧光必须了解的一些概念（Some concepts that atomic fluorescence has to understand）.docVIP

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2017-07-24 发布于河南
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原子荧光必须了解的一些概念（Some concepts that atomic fluorescence has to understand）.doc

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原子荧光必须了解的一些概念（Some concepts that atomic fluorescence has to understand）

原子荧光必须了解的一些概念（Some concepts that atomic fluorescence has to understand） The first part of the atomic fluorescence must understand some of the main points 1.. The advantages of atomic fluorescence spectrometry include: 1. Simple spectral line; high sensitivity and low detection limit; suitable for multi-element analysis. 2. the fluorescence intensity and the relationship between the measured concentration of atomic fluorescence: analysis of low concentration, a linear relationship between the simple fluorescence intensity and concentration measured concentration increases, due to line broadening, self absorption and scattering, curve bending. The intensity of the 3. atom fluorescence and the intensity of the excitation light source are only applicable in the range of the intensity of the certain excitation light source, and it is impossible to improve the detection limit by limiting the increase of the radiation intensity of the light source. 4., overcome the liquid phase and gas phase interference way: first, increase pH, increase the solubility of metal particles; second, reduce the concentration of potassium borohydride. 5. atomic fluorescence spectrometer components: hydride generator, excitation light source, optical system, atomization system and photometry system. 6. calibration of light source drift and fluctuation: re determination of blank after a certain number of samples to fit the standard curve. 7. several concepts AFS: atomic fluorescence spectrometry. Atomic vapor absorb certain wavelengths of light radiation energy is excited, excited atom in the deexcitation process emits light radiation of a certain wavelength is called atomic fluorescence detection, atomic fluorescence analysis data analysis method as atomic fluorescence spectrometry. The main role is: the current carrying and reducing agent reaction, generate nascent hydrogen (H?). Reducing agent: nascent hydrogen (H?) the main source. Atomization device: where the hydride atomization is located,