毕业论文心得研发经验（The graduation thesis research experience experience）.docVIP

毕业论文心得研发经验（The graduation thesis research experience experience） Development experience Hjd7953 I read in the Hebei Normal University of chemistry and chemical engineering research in nearly a year during the experiment error list, hope we learn a lesson. The wrong operation and the consequences of the serial number 1 SOCl2, PCl3, H2SO4 concentration, HCl concentration, ammonia containing the substance or solvent untreated directly into the sink in the laboratory The atmosphere was foul. 2 circulating pump for pumping into rotary evaporator or vacuum distillation containing SOCl2, PCl3, H2SO4 concentration, HCl concentration, ammonia etc. these substances of solvent, after not to replace the water, resulting in experimental cross contamination. 3 in a rotary evaporator vacuum distillation containing SOCl2, PCl3, H2SO4 concentration, HCl concentration, ammonia etc. these substances solvent, not timely cleaning after use rotary evaporator, or you regardless of the consequence brought on by the cross contamination. 4 before reaction, did not carefully check the instruments such as glass flask, separatory funnel have cracks, or found, luck, think nothing, especially in the system of gas pressure and even did not change significantly during the experimental process, resulting in the bottle broke experiment would have failed. The 5 experiment is always troublesome, do not wear rubber gloves (according to select different types of gloves of the reagents, not nature) with gas masks, without goggles, also do not check whether rupture with rubber gloves, the results made the skin very painful, not white is black, yellow, peeling. 6 with the oven drying did not try to drain the flask bottle of water or organic solvent to the drying box is very dangerous. 7 with a hair dryer dryer flask without the bottle to drain the water or organic solvent is not used to cool dry bulk solvent directly by hot air blow drying, so dangerous. 8 electrical equipment is broken, do not understand h