zyhx_jy0101（zyhx _ jy0101）.docVIP

zyhx_jy0101（zyhx _ jy0101） A, extraction Three to determine the polarity of the compound principle: 1. carbon containing more polar about small, containing more oxygen, higher polarity; 2. polar oxygenated compounds containing carboxyl, hydroxyl, carbonyl containing; The 3. component, acid alkaline components and amphoteric ingredients: change pH, change the existing state, changing the polarity (dissociation type free type). (a) solvent method According to the property of traditional Chinese medicine containing active ingredients and impurities coexist, select the appropriate solvent, the effective component from Chinese herbal medicine extraction using appropriate methods. 4 aspects need to grasp the problem: 1. commonly used solvents and properties The commonly used solvents including petroleum ether, benzene, chloroform, ether (Et2O) (CHCl3), ethyl acetate (EtOAc), n-butanol (n-BuOH), acetone (Me2O), ethanol (EtOH or Alc), methanol (MeOH) and water, followed by small gradual polarity. The row in n-butanol solvent before mixed with water can be layered, can be used for extraction of chemical constituents from aqueous solution, and acetone, ethanol, methanol and water after mixing layers. In addition, low boiling point such as chloroform ether heavier than water need to know some basic knowledge. A type questions: The following is the weakest polar solvent A. ethanol B. methanol C.. D. ethyl acetate E. n-butanol Answer [No. 981010101] Answer: D A type questions: The polarity of the solvent is the strongest A. ethanol B. hexane C. ether D. ethyl acetate E. chloroform Answer [No. 981010102] Answer: A A type questions: The solvent polarity, is the strongest A. methanol B. ethanol C. chloroform D. water E. ethyl acetate Answer [No. 981010103] Answer: D The polarity of the 2. chemical components of traditional Chinese Medicine The chemical constituents of traditional Chinese medicine because of the different molecular structure will show different polarity. The decisi