武大实验考试题（Wuhan University experimental examination）.docVIP

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武大实验考试题（Wuhan University experimental examination）.doc

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武大实验考试题（Wuhan University experimental examination）

武大实验考试题（Wuhan University experimental examination） First, fill in the blanks: (24 minutes, 2 minutes / empty) 1, if the reference material is not dry, the standard solution concentration will be higher. 2, a pipetting solution, when the liquid level rises to the line above, using right hand index finger _ __ block the nozzle. 4, the calibration of EDTA solution, if the control of pH=5, ___XO is often used as a metal ion indicator; if the control of pH=10, _EBT is often used as a metal ion indicator. 5. in operation in the left hand control titration burette, right hand holding the conical flask; close to the end point titration, should control the droplet to join, add half drop of solution is the solution gently rotating cock, hanging in the outlet pipe mouth, forming half drops, with the inner wall of the bottle will fall with the cone, and then wash the bottle blowing. After the titration; reading, should be under the line of sight and __ titration was to read the scale line parallel. __. 6. the total hardness of water was measured by masking the small amount of coexisting ions such as Fe3+ and Al3+ with triethanolamine. 7.NaOH standard solution absorbs CO2 because of improper preservation. If H3PO4 is titrated to second measuring points in this NaOH solution, the analysis result of H3PO4 will be higher. Two, judgment questions: (8 points / 2 points / questions) 1. to determine the hardness of water, Ca and Mg should be quantified respectively. (x) 2. for a measure, its system error is not measurable. (x) 3., the complex of metal ion indicator and metal ion is too stable, which is called the closing phenomenon of indicator. (V) 4. to the total alkalinity of HCl standard solution titration in alkaline solution, the inner wall of droplets burette, Will make the analysis result low. (V) Three, use: (68 points) 1. Why adding buffer solution in complexometric titration? (14 points) Answer: all kinds of metal ions and titrant will be allowed to produce a minimum pH valu