济南市售食用植物油中多环芳烃污染状况分析.docVIP

济南市售食用植物油中多环芳烃污染状况分析 杨晓倩 焦海涛 刘素华 曹小丽 山东省济南市疾病预防控制中心 X 关注成功！ 加关注后您将方便地在 我的关注中得到本文献的被引频次变化的通知！ 新浪微博 腾讯微博 人人网 开心网 豆瓣网 网易微博 摘????要： 目的 了解济南市售食用植物油中15种多环芳烃残留含量, 为济南市售食用油安全监管提供依据。方法采用超高效液相色谱仪 (UPLC) , 荧光检测器 (FLR) 同时快速检测植物油中15种多环芳烃残留含量。结果 150份样品中苯并 (a) 芘检出率为44.00% (66/150) , 超标率为6.00% (9/150) 。定型包装产品苯并 (a) 芘检出率为43.33% (39/90) , 无样品超标;散装产品检出率为45.00% (27/60) , 超标率为15.00% (9/60) ;苯并 (a) 芘、PAH4及PAH15含量定型包装产品均低于散装产品 (t=2.3711, P0.05;t=2.1225, P0.05;t=2.0455, P0.05) 。花生油中苯并 (a) 芘检出率为43.75% (21/48) , 超标率为6.25% (3/48) ;大豆油检出率为44.64% (25/56) , 超标率为7.14% (4/56) ;玉米胚芽油检出率为18.75% (3/16) , 无样品超标;调和油检出率为57.69% (15/26) , 超标率为7.69% (2/26) ;色拉油检出率为50.00% (2/4) , 无样品超标。不同种类样品的苯并 (a) 芘含量差异无统计学意义 (H=4.3347, P0.05) ;PAH4化合物含量和PAH15化合物含量差异有统计学意义 (H4=24.3381, P40.05;H15=22.0690, P150.05) , 结果均为花生油大豆油调和油玉米油色拉油。结论 济南市售食用植物油中存在多环芳烃污染, 应重点加强市场散装植物油的生产、运输、贮存和销售监管。定期开展多环芳烃类化合物的食品安全专项监测, 提升食品安全水平。 关键词： 食用植物油; 多环芳烃; 污染状况; 作者简介：杨晓倩 (1985-) , 女, 山东高唐人, 硕士, 主管技师, 主要从事食品理化检验工作 作者简介：曹小丽, E-mail:cxlshiwo@163.com 收稿日期：2017-01-14 Polycyclic aromatic hydrocarbons contamination investigation of vegetable oil samples in Jinan YANG Xiao-qian JIAO Hai-tao LIU Su-hua CAO Xiao-li Jinan Municipal Center for Disease Control and Prevention, Shandong; Abstract： Objective To understand the content of 15 kinds of polycyclic aromatic hydrocarbons ( PAHs) in edible vegetable oil and provide scientific basis for the safety supervision of edible oil in Jinan. Methods The concentration of PAHs in samples were determined by ultra performance liquid chromatography with fluorescence detection. Results The detection rate of benzo ( a) pyrene in 150 samples was 44. 00% ( 66/150) , and the exceeding standard rate was 6. 00% ( 9/150) . The stereotypes packaging products detection rate of benzo ( a) pyrene was 43. 33% ( 39/90) and there was no sample exceeding standard. The detection rate of bulk product was 45. 00% ( 27/60) and the exceeding standard rate was 15. 00% ( 9/60) ;the stereotypes packaging products were lowe