纯Ni中氢致开裂的透射电镜原位观察-金属学报.PDFVIP

第 37卷 第 9期 舍 扁 学 垃 V0l_37 NO9 2001 年 9 月 ACTA M ETALLURGICA SINICA Septelnber200 l 纯 Ni中氢致开裂的透射电镜原位观察 季金许 王燕斌 乔利杰 街武扬 (北京科技大学材妊物理系．北一lg10008；{) 摘 要 纯 Ni在适射电镜ITEM)中原位拉呻时．裂纹尖端首先发射太垃位错 T-~a,ftt；成尢位错 ．微裂纹在裂纹顶端适 缍形格或在无位错医中 连续形棱 并丑形援后垮钝化成孔嗣或缺FI 利用}孚蠹的恒位移加戟 白，可在 TEM 由原位研究芒氯前 后恒位移试佯裂尖位错组惑帕变化 结果表明．氧能促连也错的赘射 增疽邱运 卡u末充象纯 Ni十H比．觅茸试样在更低的外I 力下位错就会发射卅运动，当氢促进 的位错盅射卡u运动到临界条，生 就苫恒氢致裂纹形埙、扩展，导致低虚 ／J目悬断 关键词 Nj．氢致开裂．透射电镜，位错发射盯运动 中图法分类号 TGI4615．TG11521 文献标识码 A 文章编号 0412—1961(2001)Og091l一06 Ⅳ S TEM STUDY 0N HYDR0GEN-INDUCED CRACK ING 0F NICKEL LIJinau ⅣG Yanbin QIA0Lifie CltUw ∽ Dep~tmentofMateriMsPhysics，UniversityofScienceandTechnologyBeijing．Beijing100083 Correspondent：LiJinxu．1ecturer?TeLro1f】Faz：(01@623223d5 Email：lijinxu@sohuCOTY~ M anuscriptreceived 2001—01—02，inrevisedform 2001—04-23 ABsTRAcT ， situtensiletestinTEM showedthatadislocation—freezone(DFZ)formedaheadof aloadedcracktipwhendislocationemissionand motionreached equilibrium underkeepingconstant displacement．and am icrocrack initiated afterthedislocation em ission and motion developed to a certainconditionthroughincreasingload A constantdeflectiondevicedesignedforUSewithinTEM wasused toinvestigatethechangeindislocationconfigurationaheadofaloadedcracktipbeforeand afterhydrogen—chargingandcrackinitiationduringchargingunderconstantdisplacement．Theresults showed thathydrogen couldenhancedislocation emission，multiplication and motion A hydrogen- inducedcrackwouldinitiateduringchragingunderconstan~displagementwhenthehydrogen~enhanced dislocation emissionandmotiondevelopedt0acriticalcondition KEY W oRDS nicke1．hydrogen-inducedcracking，TEM ．dislocationemissionandmotion 原子氢能使纯 i的拉伸塑陛大大下降．在恒载荷下 使塑生l区中的应变增大 金相原位观察发