SIMA制程中不同应变量及加热条件对AZ61镁合金微观组织之-Yoke.PDFVIP

SIMA製程中不同應變量及加熱條件對AZ61鎂合金微觀組織之影響 Effects of different strain and heating factor on the microstructure of AZ61 Mg alloy produced by SIMA process 葉怡良* 、呂傳盛、陳立輝、洪飛義 國立成功大學材料科學及工程學系 Yi-Liang Ye*, Truan-Sheng Lui, Li-Hui Chen, Fei-Yi Hung Department of Materials Science and Engineering, National Cheng Kung University. *Email: hahaha7603@ Tel : 886-6-2757575 ext 62964 摘要 本研究利用不同應變量之AZ61鎂合金擠型材經應變導引熔漿活化法(Strain Induced Melt Activation, SIMA)製程後，探討其微觀組織的演變。SIMA製程具發 展潛力因成形過程簡便、設備裝置較為單純，所以成本較為低廉。本研究藉由不 同擠形比去取代傳統利用冷壓縮所導入的應變量並探討其不同擠形比對微觀組 織之影響。藉由提升加熱溫度及適當的持溫時間獲得較等軸之晶粒，本研究發現 擠形量EX3.5材其加熱溫度560℃ 、持溫15分鐘為最佳結果其平均晶粒徑約為 70.3μm 、液相率約20.2 ，EX2.5材則加熱溫度560℃、持溫20分鐘為最佳結果，平 均晶粒徑約為67.9μm 、液相率約17.3故應變量大(EX3.5)的材料其液相較易生成並 包覆固相晶粒，進而縮短球化時間。晶粒粗大化機制在加熱初期由coalescence所 主導，後期則由Ostwald ripening所主導，且藉由Lifshitz-Slyozov-Wagner LSW理 論分析晶粒粗大速率。 關鍵詞：半固態製程, SIMA, AZ61 Abstract Strain-induced melt activation (SIMA) is a process with development potential due to its simplicity and low cost. The semisolid billet of AZ61 Mg alloy was fabricated by the modified SIMA process which was applied with different extrusion ratios instead of the conventional cold compression. The grain becomes more globular with increasing the reheating temperature and the appropriate holding time. Moreover, EX3.5 has the optimal heating parameters for holding temperature 560℃ and heating time 15 minutes. EX2.5 has the optimal heating parameters for holding temperature 560 ℃ and heating time 20 minutes. Therefore, large strain (EX3.5) material generated liquid phase easily and shorted the heating time. The dominant mechanism of grain coarsening at initial stage is grain coalescence, while Ostwald ripening at longer holding time, and the coarsening rate was analyzed by LSW (Lifshitz-Slyozov-Wagner) theory. Key word: Semisolid process, SIMA, AZ61