溶胶-凝胶法在3D-SiC陶瓷表面制备纳米MgO薄膜-Journalof.PDF

第31 卷第8期 东 北 大 学 学 报 ( 自 然 科 学 版 ) Vol31, No. 8 2 0 10 年 8 月 Journal of Northeastern U ni ersity( Natural Science) Aug. 2 0 1 0 - 3D-SiC MgO 喻 亮, 马娅娜, 茹红强, 岳新艳 ( , 110004) : Mg( NO ) 6H O , , , - 3 2 2 MgO , - ( 3D-SiC) MgO , MgO X ( XRD) ( SEM) , HF 3D-SiC m ( Mg( NO ) 6H O)m ( ) = 10 3 2 2 MgO , 80 10 min, 480 10 min, 800 1 h, , 08~ 10 m MgO , MgO 500 nm : MgO ; - ; ; : O 484 : A : 1005-3026( 2010) 08- 112 1-05 Preparation of MgONanofilm on Surface of 3D-SiCby So-l Gel Method YU L iang , MA Ya-na, R UH ong-qiang, Y UE X in-yan ( Key Laboratory for Anisotropy and T exture of Materials, Ministry of Education, Northeastern Uni ersity, Shenyang 110004, China. Correspondent: RU Hong-qiang , E-mail: ruhq @ smm. neu. edu. cn) Abstract: With Mg ( NO ) 6H O, anhydrous ethanol and collodion emulsion used as starting 3 2 2 materials, sol ent and surfactant, respecti ely, the M gO sol w as prepared by so-l gel method. T hen the MgO sol was coated on the surface of the ceramic skeleton of 3D-SiC by dip-coating process to get MgO nanofilm after roasting. The phase composition and microstructure of the nanofilm w ere in estigated ia XRD and SEM . T he results show ed that the smooth and compact M gO nanofilm w hose thickness ranges from 0. 8 to 1. 0 m can be deposited on the surface of 3D- SiC as substrate the w ay the substrate should be eroded in HF solution for 30 min to make sure that the coated M gO sol has the mass ratio of M g( NO3) 2