预应变对DP600钢氢脆敏感性的影响-中国腐蚀与防护学报.PDF

第38 卷 第5 期 中国腐蚀与防护学报 Vol. 38 No. 5 2018 年10 月 Journal of Chinese Society for Corrosion and Protection Oct. 2018 预应变对DP600 钢氢脆敏感性的影响 柯书忠 刘 静 黄 峰 王 贞 毕云杰 武汉科技大学 省部共建耐火材料与冶金国家重点实验室 武汉 430081 摘要 利用慢应变速率拉伸实验(SSRT) 及双电解池渗氢实验，结合断口形貌观察和分析，探索了预应变对 DP600 钢氢脆敏感性的影响规律及机理。结果表明：在本实验预应变量范围内，预应变量小于15%时，随着预 应变量的增大，DP600 钢试样的氢脆敏感性不断增大，当预应变量达到15% 以后，其氢脆敏感性基本趋于稳 定。预应变增大了钢中的位错密度，使氢的有效扩散系数降低，有效捕获的氢量增加，从而使钢试样的氢脆敏 感性增大；但当预应变量进一步增加至15% 以上时，位错的相互缠结减缓氢的扩散和聚集速度，从而使试样的 氢脆敏感性增加趋于平缓。 关键词 DP600 钢 预应变 慢应变速率拉伸实验 渗氢技术 氢脆敏感性 氢扩散 中图分类号 TG 171 文章编号 1005-4537(2018)05-0424-07 Effect of Pre-strain on Hydrogen Embrittlement Susceptibility of DP600 Steel KE Shuzhong, LIU Jing, HUANG Feng, WANG Zhen, BI Yunjie State key Laboratory of Refractories and Metallurgy, Wuhan University of Science and Technology, Wuhan 430081, China Correspondent: LIU Jing, E-mail: liujing@wust.edu.cn Supported by National Natural Science Foundation of China Manuscript received 2017-10-11, in revised form 2017-11-07 ABSTRACT The effect of pre-strain on the hydrogen embrittlement (HE) susceptibility of DP600 steel was studied by means of slow strain-rate tensile (SSRT) test, electrochemical permeation technique and fractograph observation of fracture surface. The results indicate that the HE susceptibility of DP600 steel increases with the increasing pre-strain when the level of pre-strain is below 15%, and then tends to sta- ble when the pre-strain exceeds 15%. The pre-strain increases dislocation density and the amo