光纤式后向散射纳米颗粒测量装置研究-电气工程专业论文.docxVIP

山东理工大学硕士学位论文摘要 山东理工大学硕士学位论文 摘要 I I 摘 要 针对传统动态光散射法无法测量高浓度溶液中纳米颗粒粒径问题，本文通过分析 动态光散射的时域自相关理论，研制出基于后向动态光散射法的一体化光纤探头，克 服了传统动态光散射法的缺陷。本文主要研究内容如下： 1、传统动态光散射法测量纳米颗粒溶液时，多重散射效应往往在相对较低的浓 度时就开始显现其影响，因此开发可用于检测高浓度纳米颗粒的动态光散射技术首先 应着眼于减弱多重散射影响。 2、本文采用减小散射光程的方法来减弱多重散射影响，并研究光纤探头空间相 干性问题。通过对影响空间相干性的几个因素（空间相干角、相干面积以及散射体积） 进行分析得出提高光纤探头相干性的方法。 3、依据满足空间相干性的判据，在分析光纤探头结构参数的基础上，给出后向 散射式光纤探头结构参数的最优设计方法。 利用本文设计的光纤式一体化探头，分别对不同浓度的标准颗粒溶液进行测量， 测量结果表明本文设计的光纤式后向散射纳米颗粒测量装置，不仅能够测量低浓度溶 液，而且也能测量传统装置不能测量的高浓度溶液，由于探头设计符合空间相干性要 求，因此输出信号的信噪比高，测量结果相对偏差5%，测量重复性5%，较传统设 备更加准确。 关键词：光纤探头；后向散射；纳米颗粒测量；空间相干性 山东理工大学硕士学位论文Ab 山东理工大学硕士学位论文 Abstract II II Abstract Because the traditional dynamic light scattering method cant measure the nano particle size in high concentration solution. Through the analysis of the time domain correlation theory of the dynamic light scattering, we developed a kind of integrated optical fiber probe based on the backward dynamic light scattering method. This kind of probe overcomes the defect of the traditional dynamic light scattering method. In this paper, the main research contents are as follows: 1, When we use the traditional dynamic light scattering method to measure the size of nano particles solution, the effects of multiple scattering began to show its effects in relatively low concentration. So the key to develop a kind of dynamic light scattering technique that can be used for detecting high concentration of nano particles is to weak the influence of multiple scattering . 2, This paper uses the method of reduced scattering path to weaken the influence of multiple scattering, and studies on optical fiber probe spatial coherence. By analyzing the factors that influence the spatial coherence (spatial coherence angle, coherence area and scattering volume) to find the method that can improve the coherence of the optical fiber probe. 3, According to the criterion of satisfy the spatial coherence and based on the analysis of the structure parameters of the fiber probe, the optimum design me