重铬酸钾容量法中不同加热方式测定土壤有机质的比较-浙江农业科学.PDF

浙江农业学报 （）： ， Acta Agriculturae Zhej iangensis 17 5 311 ～ 313 2005 重铬酸钾容量法中不同加热方式测定土壤有机质的 比较研究 季天委 （浙江省农业厅 土肥站，浙江 杭州 310020 ） ［］ 2 摘 要：以油浴加热法 测定土壤有机质含量结果为基准，比较30 min 或60 min 100℃恒温水浴加热法和稀 释水合热法测定有机质的精确度和准确度，并获得三者的氧化校正系数平均值分别为 ， 和 。结 1. 16 1. 13 1. 33 果表明， 恒温水浴加热—重铬酸钾容量分析法，可达到经典油浴加热法的测定精度和准确度，而且操 30 min 作简便，是可靠的土壤有机质含量测定方法。 关键词：土壤；有机质；重铬酸钾法；恒温水浴加热法；氧化校正系数 中图分类号： + 文献标识码： 文章编号： （ ） S153 .6 21 A 1004 - 1524 2005 05 - 0311 - 03 Comparison on determining the organic matter contents in the soils by different heat- ing methods in the potassium dichromate-volumetric method JI Tian-wei （ ， ， ， ） Soil and Fertilizer Station Agricultural Dep artment of Zhej iang Province Hangzhou 310020 China ： Abstract The precisions and accuracies of the soil organic matter contents tested by three heating methods including the boiling water bath heating 30 min or 60 min and the dilution heating method were compared with the oil bath heating method as a standard conventional method . The results showed that the oxidation adjusting coefficients for above three heating method were 1. 16， ， ， 1. 13 and 1. 33 respectively . The precision and accurycy of the boiling water bath heating method were as the same as the oil bath heating method in determining soil organic by the potassium dichromate-volumetric method . Because the boiling water bath heating 30 min method is facility and credib