可视化优化超临界CO2萃取茶树花精油工艺-经济学家.PDF

※工艺技术 食品科学 2015, Vol.36, No.12 65 可视化优化超临界CO 萃取茶树花精油工艺 2 1 , 1 * 1 1 1 2 许 静 ，孙益民 ，邹 莉 ，方追追，纵 看 ，王 举 （1.安徽师范大学化学与材料科学学院，功能性分子固体教育部重点实验室，安徽 芜湖 241000 ； 2.安徽瑞研新材料技术研究院，安徽 芜湖 241000 ） 摘  要：采用超临界CO2 技术对茶树花精油的萃取进行较为系统研究。选择萃取压力、萃取温度、静态萃取时 间、动态萃取时间及分离温度5 个影响因素，以萃取量为试验指标，运用多因素多水平可视化设计法安排试验， 以多因素多水平可视化优化法对试验数据进行分析优化，得到优化的工艺范围：萃取压力19～22 MPa 、萃取温度 50～60 ℃、静态萃取时间30～50 min 、动态萃取时间80～100 min、分离温度40～50 ℃。3 组验证实验得到的萃取 物质量在优化区内8 g 以上，研究证明多因素多水平可视化优化方法可以实际应用。 关键词：超临界CO2萃取；茶树花；多因素多水平可视化优化 Visual Optimization of Extraction Process of Tea Flower Oil with Supercritical Carbon Dioxide 1 1,* 1 1 1 2 XU Jing , SUN Yimin , ZOU Li , FANG Zhuizhui , ZONG Kan , WANG Ju (1. Key Laboratory of Functional Molecular Solids, Ministry of Education, College of Chemistry and Materials Science, Anhui Normal University, Wuhu 241000, China; 2. Anhui Rereasearch Institute of New Materials Technology, Wuhu 241000, China) Abstract: This paper reports a systematic investigation of the supercritical carbon dioxide extraction of essential oil from tea flower. Extraction pressure, temperature, static extraction time, dynamic extraction time and separation temperature were chosen as main variables influencing extraction efficiency. The multifactor and multilevel visual design method (m2VD) was applied to design the experiments and the experimental data were analyzed by the multifactor and multilevel visual optimization method (m2VO) to optimize the extraction condi