冶金专业毕业设计--年产1000t仲钨酸铵生产车间设计.docVIP

冶金专业毕业设计--年产1000t仲钨酸铵生产车间设计 摘 要 本文是以白钨精矿为原料年产1000吨APT 仲钨酸铵 生产车间的设计说明书按照一般有色冶金生产车间设计的步骤文章首先介绍了APT生产的的现状结合原料特征通过对APT整个工艺过程生产方法的比较选择了NaOH高压浸出分解白钨精矿离子交换法除杂和转型选择沉淀法分离钨钼蒸发结晶生产APT通过对各生产工序金属平衡物料平衡计算和设备选型确定了各工序所需原料的量和设备的型号规格和数目并进行了合理的车间配置通过分析生产过程中工业三废的产生和危害提出了三废处理的方案根据生产过程需要对车间进行了劳动定员进而对整个工艺过程进行了技术经济分析计算结果表明本设计所采用工艺流程技术上可行经济上合理 「关键词」 白钨精矿 NaOH高压浸出 离子交换 APT 设计 Abstract The specification is a workshop of 1000ty Ammonium paratungstate APT produced with scheelite concentrates Following the general design steps of nonferrous metallurgy workshop the present situation of the APT production was first presented According to the characteristics of the raw material technological process of sodium hydroxide NaOH leaching at high pressureion exchangeselectively precipitation to separate Moevaporation and crystallization process was selected as the process of APT production The quantity of various materials in every process were fixed up and the corresponding equipments were designed or selected include the type size and number originated from the result of calculating of the balance of metal and matter The workshop is reasonably designed The strategy of dealing with the industrial waste was proposed following the analysis of the source and the harm of the waste The work force was arranged according to the requirement of producing process At last the economic target was analyzed All these results shows that the process of this design is reasonable and economical Keywords Scheelite concentrates sodium hydroxide leaching at high pressure ion exchange ammonium paratungstate design 文献综述 钨冶金概况 自1781年由瑞典化学家舍勒发现以来钨以其具有熔点高硬度大耐磨和耐腐蚀等优良性能而得到广泛应用在冶金机械石油化工航空航天和国防工程等诸多领域中有着极其重要的地位 在解放之前中国的钨冶炼处于空
但新中国成立后从20 世纪50 年代苏联援建的黑钨精矿苏打烧结净化除杂白钨沉淀钨酸煅烧制取三氧化钨的冶炼工艺开始我国钨冶炼技术走上了工业化生产的道路并针对我国钨精矿资源的特点我们自主开发了白钨精矿经典工艺制取仲钨酸铵的工业项目20 世纪80 年代以来先进的离子交换和溶剂萃取技术在钨冶炼生产中得到广泛应用黑钨精矿碱压煮溶剂萃取蒸发结晶和黑钨精矿碱压煮离子交换蒸发结晶制取仲钨酸铵新工艺的采用标志着我国钨冶炼工业开始向世界先进行列迈进但是经过20多年的发展中国钨业迎来了自己辉煌的成果在若干个技术领域已经能够和世界先进国家媲美某些技术已经是世界的先