《Zr基块体金属玻璃和复合材料样品的研究》》-毕业论文（设计）.docVIP

沈阳理工大学学士学位 PAGE PAGE 25 摘 要 本文利用液态浸渗铸造法制备了W球/Zr基非晶复合材料，其中增强体W球由W颗粒和粘结剂烧结而成，直径分别为1毫米和2.8毫米。利用XRD和SEM分析了Zr基非晶合金和W球/Zr基非晶复合材料的微观结构。对Zr基非晶合金的热稳定性进行了差热分析。利用SEM观察了Zr基非晶合金和W球/Zr基非晶复合材料的压缩断口形貌和剪切带的变化。测试了非晶基体和增强体W球的显微硬度。研究了复合材料在应变速率为1×10-4s-1和1×10-2s-1下的室温压缩变形行为。结果表明，W球/Zr基非晶复合材料的塑性明显优于纯非晶合金的塑性。W球一方面阻碍了剪切带的扩展，另一方面促进了多剪切带的产生。但是，和纯非晶合金相比，复合材料的强度有所降低。在同一应变速率，1mm W球/Zr基非晶复合材料的塑性要比2.8mm W球增强的好。在不同应变速率下，1mm W球/Zr基非晶复合材料在低应变速率下的塑性较好。 关键词：非晶合金；复合材料；W球；压缩性能；应变速率 Abstract The Zr-based bulk metallic glass composites reinforced by the W powder sinter balls with a size of 1mm and 2.8mm in diameter were prepared using infiltration technique．The structure of the Zr-based bulk metallic glass and the Zr-based bulk metallic glass composites were characterized by X-ray diffiraction and Scanning election microscope．The heat stability of the Zr-based bulk metallic glass was analysied by DSC．The fracture surfaces and shear bands were examined by SEM．In addition, The microhardness of bulk metallc glass and W balls was tested．The compressive deformation behaviours of the composites at two strain rates of 1×10-4s-1 and 1×10-2s-1 were investigated on the room temperature．The results show that the plasticity of Zr-based bulk metallic glass composites is obviously enhanced when compared with bulk metallic glass．It is attributed to the effect of W balls，which constrain shear bands propagation and promote the formation of multiple shear bands；while，the compressive strength reduces for the two kind of composites when compared with bulk metallic glass．The plasticity of the composite reinforced by W balls with a diameter of 1 mm is better than that with a diameter of 2.8 mm at the same strain rate．The plasticity of the composite reinforced by W balls with a diameter of 1 mm at the rate of 1×10-4s-1 is higher than at the rate of 1×10-2s-1． Keywords：metallic glass；composite；W balls；compressive properties；strain rate 目 录 TOC \o 1-3 \h \z \u 摘 要 I Abstract II 1 绪论 1 1.1非晶合金概述 1 1.1.1