《三氯氢硅、四氯化硅的提纯》-毕业设计（论文）.docVIP

PAGE 1 三氯氢硅、四氯化硅的提纯 第 PAGE I 页 南京化工职业技术学院 毕业论文（设计） 课 题 三氯氢硅、四氯化硅的提纯 系 部 化学工程系 专 业 高分子材料成型加工技术 与物流管理 班 级 高材与物流0552 学 号 0501270210 姓 名 导 师 定稿日期： TIME \@ yyyy年M月d日 2015年1月6日 PAGE 1 第 PAGE II 页 三氯氢硅、四氯化硅的提纯 摘 要 超纯硅质量的好坏，往往取决于原料的纯度。超纯硅的发展方向是如何进一步提高纯度效果。精馏法是一种最重要的提纯方法，此法具有处理量大，操作方便，板效率高，又避免引进任何试剂，绝大多数杂质都能被完全分离，特别是非极性重金属氧化物。精馏塔的操作是从物料平衡、气液平衡、热量平衡及精馏塔性能等几个方面考虑，通过控制系统建立并调节塔的操作条件，使精馏塔满足分离要求。分离效率和处理能力是调节精馏塔的主要目的，对此我们进行一个理论结合实际的研究。通过对精馏塔结构的理解和控制参数之间的联系，采用智能计算机操作系统对精馏塔的各项参数进行控制，从而使组分分离出的产品达标。 关键词：三氯氢硅,四氯化硅,精馏,精馏塔,控制参数,回流比 Abstract good or bad the quality of ultrapure silicon, often depends on the purity of raw materials. The direction of development of ultra-pure silicon is how to further improve the purity of the effect. Distillation is one of the most important purification methods, this method has a deal with large, easy to operate, high efficiency plate, but also to avoid the introduction of any reagents, the vast majority of impurities can be completely separated from the heavy metal oxides in particular non-polar. Distillation column operation are from the material balance, vapor-liquid equilibrium, heat balance and distillation performance aspects to consider, through the control system set up and adjust the tower operating conditions, so that distillation column satisfy the separation requirements. Separation efficiency and the ability to deal with the main purpose of regulation of distillation, which we carried out a theoretical combination of the actual research. Structure of the distillation column through the understanding and control parameter the link between the use of smart computer operating system on the parameters of distillation column control, so that isolated components of the Product standards. Keywords: trichlorosilane, tetrachlorosilane, rectif