HJ 1074-2019 水质 三丁基锡等 4种有机锡化合物的测定 液相色谱-电感耦合等离子体质谱法.pdfVIP

Water quality—Determination of four organic tin compounds including tributyltinLiquid chromatography/inductively coupled plasma mass spectrometry ii 1 1 2 1 3 1 4 1 5 2 6 3 7 4 8 5 9 6 10 7 11 7 12 7 A 8 B 9 i 4 4 - AB 2020630 ii 4 - 1000 ml1.0 ml20.0 μl 0.004 μg/L0.005 μg/L0.016 μg/L0.020 μg/L 20.0 μl 3 μg/L6 μg/L12 μg/L24 μg/L A HJ 91.1 HJ 442 HJ 493 HJ/T 91 HJ/T 164 CH3CN CH3COOH 1 C H N 6 15 CH3OH CH COCH 3 3 CH Cl 2 2 NaCl 400 2 h ρ HCl =1.19 g/ml 1+1 50.0 ml 4.8 100 ml 1+19 50.0 ml 4.8 1000 ml 1+99 1.0 ml 4.8 100 ml Na SO