HJ 1071-2019 水质 草甘膦的测定 高效液相色谱法.pdfVIP

Water qualityDetermination of glyphosate High performance liquid chromatography ii 1 1 2 1 3 1 4 1 5 1 6 2 7 3 8 3 9 4 10 5 11 6 12 7 i 2020630 ii 20 μl 2 μg/L8 μg/L HJ 91.1 HJ/T 91 HJ/T 164 pH 49 9- FMOC-Cl CH3CN CH3OH CH Cl 2 2 1 ρ HCl =1.19 g/ml ρ H PO =1.69 g/ml 3 4 NaOH 1+1 50 ml5.4 50 ml c NaOH 0.1 mol/L 0.4 g5.6 100 ml φ H PO =0.2% 3 4 2.0 ml5.5 1000 ml Na C H O ·2H O