毕业设计(论文)-年产10000吨苯乙酮生产工艺设计.doc

毕业设计(论文)-年产10000吨苯乙酮生产工艺设计.doc

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哈尔滨工业大学工学硕士学位论文 哈尔滨理工大学学士学位论文 - PAGE II - - PAGE I - 年产10000吨苯乙酮生产工艺设计 摘 要 苯乙酮是一种重要的化工原料,也是合成其他香料的重要中间体,主要用途有:1、作溶剂;2、作香料;3、用于合成苯乙醇酸、α--苯基吲哚和异丁苯丙酸等,也用作塑料的增塑剂;4、可用于医药,有催眠性。、 目前工业上采用乙苯空气直接氧化法制取苯乙酮。该方法转化率不高、选择性差,有待改进。由乙苯氧化制取苯乙酮对石油化工下游产品的开发,精细化工的发展具有重要的意义。 本设计通过对反应原理以及氧化法生产工艺的分析,确定了年产10000吨CEVA的简要工艺流程,并根据绘图标准,绘制了带控制点的分散工艺流程图。同时,按照工艺流程,综合安全及操作方便等因素,利用AutoCAD2007绘制了厂房布置图。通过进行物料衡算和热量衡算,确定了主要设备的尺寸及型号,绘制了氧化反应釜和填料塔结构图。 关键词 苯乙酮;氧化法;物热料衡算;工艺设计 全套图纸加扣?3012250582 The CEVA process design with an annual output of 10000 tons Abstract The Chinese name of CEVA is vinyl chloride-vinyl acetate copolymer, and it's prepared by the chlorinated EVA. CEVA is a kind of new polymer materials that develops up from the 1980s. At present, our country is mainly used carbon tetrachloride as a solvent of the chlorinated solvent production of the CEVA. However, carbon tetrachloride pollute the environment, and thus, its application is limited by the Montreal Protocol. Therefore, study on the non-solvent method of CEVA production technology is extremely important. In this design, I take environment protection, energy savings and lower cost into consideration, and finally select the aqueous suspension to produce the CEVA. The technology of aqueous suspension in the foreign has become increasingly mature, and because this method does not use organic solvents, the process is short, the cost is low, the pollution to the environment is little, development of this method has good prospects. But, this method needs to solve the problems of equipment corrosion and waste disposal. Based on the analysis of the principle as well as the production process of aqueous suspension method, the design identifies the brief process of an annual output of 1500 ton's CEVA. And according to the drawing standards, I draw the flow diagram of the dispersion process and chlorination process with control points. And then, in accordance with the process, considering the safety operating conv

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