AOAC998.01-国外标准规范.pdf

RESIDUES AND TRACE ELEMENTS Multiresidue Gas Chromatographic Method for Determining Synthetic Pyrethroid Pesticides in Agricultural Products: Collaborative Study ANG T L OURNAL OF NTERNATIONAL OL O P E A .: J AOAC I V . 82, N . 1, 1999 GUO-FANG PANG, YAN-ZHONG CAO, CHUN-LIN FAN, JIN-JIE ZHANG, and XUE-MIN LI Qinhuangdao Import and Export Commodity Inspection Bureau, 61 Haibin Rd, Qinhuangdao, Hebei, P.C. 066002, People’s Republic of China Collaborators: X.-G. Chu; W.-Z. Duan; X.-M. Gao; X.-Z. Hu; A. Kamel; R. Kubinec; A.Q. Lin; L.-Y. Lin; S.-M. Liu; E. Papadopoulou-Mourkidou; J. Mu; J.W. Pan; J.R. Pardue; C.H. Parfitt; G. Pavoni; M.A. Saleh; J.J. Shao; W.B. Song; S. Tahotna; J. Tekel; M.-C. Tsai; D.N. Wang; K.-O. Wang; S.S. Wong; J.X. Yu; Y. Zhou; G.-N. Zhu Fourteen laboratories from 6 countries and regions 101.5%, respectively. Reproducibility relative stand- participated in an international collaborative study ard deviation values ranged from 6.46 to 17.74%, to evaluate a multiresidue gas chromatographic from 5.94 to 18.13%, and from 5.59 to 10.48%, respec- (GC) method for determining 8 synthetic pyrethroid tively. Repeatability relative standard deviation values pesticides in grains, fruits, and vegetables. The ranged from 6.34 to 10.84%, from 5.19 to 11.72%, and study design was based on Youden’s matched- from 3.20 to 8.09%, respectively. The multiresidue GC pairs principle for collaborative tests of analytical method for determining synthetic pyrethroid pesti- methods. Each laboratory analyzed 12 collabora- cides in agricultural products has been adopted first tive samples of wh