epamethod3010a最新分析和总结.pdf

METHOD 3010A ACID DIGESTION OF AQUEOUS SAMPLES AND EXTRACTS FOR TOTAL METALS FOR ANALYSIS BY FLAA OR ICP SPECTROSCOPY 1.0 SCOPE AND APPLICATION 1.1 This digestion procedure is used for the preparation of aqueous samples, EP and mobility-procedure extracts, and wastes that contain suspended solids for analysis, by flame atomic absorption spectroscopy (FLAA) or inductively coupled argon plasma spectroscopy (ICP). The procedure is used to determine total metals. 1.2 Samples prepared by Method 3010 may be analyzed by FLAA or ICP for the following: Aluminum Magnesium *Arsenic Manganese Barium Molybdenum Beryllium Nickel Cadmium Potassium Calcium *Selenium Chromium Sodium Cobalt Thallium Copper Vanadium Iron Zinc Lead * Analysis by ICP NOTE: See Method 7760 for the digestion and FLAA analysis of Silver. 1.3 This digestion procedure is not suitable for samples which will be analyzed by graphite furnace atomic absorption spectroscopy because hydrochloric acid can cause interferences during furnace atomization. Consult Method 3020A for samples requiring graphite furnace analysis. 2.0 SUMMARY OF METHOD 2.1 A mi