epamethod3005a最新分析和总结.pdf

METHOD 3005A ACID DIGESTION OF WATERS FOR TOTAL RECOVERABLE OR DISSOLVED METALS FOR ANALYSIS BY FLAA OR ICP SPECTROSCOPY 1.0 SCOPE AND APPLICATION 1.1 Method 3005 is an acid digestion procedure used to prepare surface and ground water samples for analysis by flame atomic absorption spectroscopy (FLAA) or by inductively coupled argon plasma spectroscopy (ICP). Samples prepared by Method 3005 may be analyzed by AAS or ICP for the following metals: Aluminum Magnesium Antimony** Manganese Arsenic* Molybdenum Barium Nickel Beryllium Potassium Cadmium Selenium* Calcium Silver Chromium Sodium Cobalt Thallium Copper Vanadium Iron Zinc Lead * ICP only **May be analyzed by ICP, FLAA, or GFAA 1.2 When analyzing for total dissolved metals filter the sample, at the time of collection, prior to acidification with nitric acid. 2.0 SUMMARY OF METHOD 2.1 Total recoverable metals - The entire sample is acidified at the time of collection with nitric acid. At the time of analysis the sample is heated with acid and substantially reduced in volume. The digestate is filter