欧洲分析化学组织Eurachem 定性试验的内部质量控制：催泪瓦斯武器中活性物质的鉴定.pdf

1 Overview 1. Introduction 2. Aim 3. Portuguese legislation 4. Qualitative test procedure 5.1. Qualitative test validation: Chromatography 5.2. Qualitative test QC: Chromatography 6.1. Qualitative test validation: MS 6.2. Qualitative test QC: MS 7. Conclusion 2 1 1. Introduction Quantitative measurements involve a previous qualitative assessment (…) This stage is more obvious in separation methods of analysis. 3 1. Introduction Accreditation of chemical tests ISO/IEC 17025:2005 - General requirements for the competence of testing and calibration laboratories The results of qualitative and quantitative tests must be proven valid. Some guidelines and references for the assessment of 4 qualitative tests are available (…) 2 1. Introduction Accreditation of chemical tests (…) ILAC G17:2002: Introducing the concept of uncertainty of measurement in testing in association with the application of the standard ISO/IEC 17025 3. Only uncertainty of measurement in quantitative testing is considered for the time being. A strategy on handing results from qualitative testing has to be developed by the scientific community. 5 2. Aim Presentation of a strategy for the validation and quality control of the identification of the active substance in tear gas sprays. 6