纳米压痕法测定NiTi形状记忆合金表面氧化膜纳米硬度和弹性模量.docxVIP

HotWorkingTechnology2019,Vol.48,No.6

???????NiTi????????????????????

???1,2,??1,???1,???2

(1.??????????,????210000;2.???????????????,????210000)

??：????????NiTi???????????；???????????????????????。????：????????2、4h?，???????????，????????????????????，????700℃，????；??????600、700℃?，???????????，???4、2h，????????，???????????????????????????；?????????????（H/E?H3/E2）??????。

???：NiTi??????；???；????；????；????DOI:10.14158/j.cnki.1001-3814.2019.06.043

?????：TG174；TG115.2 ?????：A ????：1001-3814(2019)06-0182-06

MeasurementofNanoHardnessandElasticModulusofSurfaceOxidationFilmonNiTiShapeMemoryAlloybyNano-indentationWANGLibin1,2,QINLi1,WENJiqin1,DINGXifeng2

(1.JiangsuInstituteofMedicalDeviceTesting,Nanjing210000,China;2.SchoolofMaterialsScienceandEngineering,NanjingUniversityofScienceandTechnology,Nanjing210000,China)

Abstract：TheoxidationfilmonsurfaceofNiTishapememoryalloywaspreparedbyhightemperatureoxidation,andthenanohardnessandelasticmodulusoftheoxidefilmweremeasuredbynano-indentation.Theresultsshowthatwhentheoxidationtimeis2hand4h,withtheoxidationtreatmenttimeincreasing,thenanohardnessandelasticmodulusoftheoxidefilmsfirstdecreaseandthenincrease,theyreachthepeakatabout700℃,thendecrease.Whenthesubstratetemperatureis600℃and700℃,theoxidationtimehasathreshold,whichis4hand2h,respectively.Morethanthethreshold,thenanohardnessandelasticmodulusoftheoxidefilmincreasesignificantlywiththetimeincreasing.Theeffectofoxidationtreatmenttimeontheresistanceplasticity(H/EandH3/E2)oftheoxidefilmisnotsignificant.

Keywords：NiTishapememoryalloy(NiTiSMA);oxidefilm;nano-indentation;nanohardness;elasticmodulus

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