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CEM333
InstrumentalAnalysis
SimonJ.Garrett
Room:CEM234
Phone:3559715ext208
E-mail:garrett@
Lectures:Tuesday,Thursday9:00-9:50amRoom136
OfficeHours:Tuesdays10:00-11:00am
CEM333page1.1
CourseObjectives
Teachfundamentalsofinstrumentalanalysis
Lecture:Discusstheoryandbackgroundfor
(1)chemical/physicalpropertymeasured
(2)originofchemical/physicalproperty
(3)instrumentdesignandnatureofresponse
(4)signalprocessingandrelationshipbetweenreadout
topropertymeasured
Laboratory:Provideshands-onexperiencein
(1)relatinglecturematerialtopracticalanalysis
(2)designandoperationofarealinstrument
(3)measurementsonrangeofinstruments
(4)exampleanalysestoillustratevalueoftechnique
CEM333page1.2
Introduction(Chapter1)
ClassificationofAnalyticalMethods
Qualitativeinstrumentalanalysisisthatmeasuredproperty
indicatespresenceofanalyteinmatrix
Quantitativeinstrumentalanalysisisthatmagnitudeofmeasured
propertyisproportionaltoconcentrationofanalyteinmatrix
Speciesofinterest
Allconstituents
includinganalyte.
Matrix-analyte
=concomitants
Oftenneedpretreatment-chemicalextraction,distillation,
separation,precipitation
(A)Classical:
Qualitative-identificationby
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