D8discaver演讲.pptVIP

General Area Detector Diffraction System(GADDS)-D8DISCOVER a. The fast speed : The speed of data collection with an area detector can be 104 times faster than with a point detector and about 100 times faster than with a linear position-sensitive detector. 2.System configuration of The X-ray Generator Goniometer and X, Y, Z sample Stages Sample Alignment and Monitor Systems * 1. General introduction 2. System configuration 3. Basic System Operation 4. Script Files 5. XRD Evaluation Program 6.Matters needing attention and Problems 7.样品的制备和研究方式、方法 1.General introduction General Area Detector Diffraction System (GADDS), introduced by Bruker AXS, Inc., is the most advanced X-ray diffraction system in the world. The core of GADDS is the high performance two-dimensional(2D) detector Bruker AXS HI-STAR area detector. HI-STAR is the most sensitive area detector, a true photon counter in a large area. Characterization: a. The fast speed b. More information but the result in practice: The speed of data collection with an area detector can be 10~100 times faster than with a point detector(20s : 10min), not considering integration b. More information: The data has large dynamic range and 2D diffraction information. Compared to one-dimensional diffraction profiles measured with a conventional diffraction system, a 2D image collected with GADDS contains far more information for various applications. By introduction of the innovative two-dimensional X-ray diffraction (XRD 2 ) theory, GADDS has opened a new dimension in X-ray powder diffraction. Pinhole Collimator specification(mm): 0.05, 0.1, 0.2, 0.3, 0.5, 1.0 Comparison between single pinhole collimator and double pinhole collimator in terms of intensity gain, beam divergency angle ( ? ), and beam spot size on sample (D). Monocapillary specification(mm): 0.3mm That is, X-rays can be reflected by a smooth surface when the angle of incidence is smaller than the critica