德国ELMENTAR公司liquiTOC II说明书:Chap-6-分析模式.docVIP

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德国ELMENTAR公司liquiTOC II说明书:Chap-6-分析模式.doc

德国ELMENTAR公司liquiTOC II说明书:Chap-6-分析模式

Description of the analysis modes分析模式的描述 The requested analysis mode can be selected under System / Mode. 在System/Mode下,选择要求的分析模式 The actual processes will be displayed on the PC in the status field under Process, e.g. Standby or Peak processing etc. 在“Process”下, PC显示出实际执行过程.。例如:“Standby”或“Peak processing”等。 TC Mode 总碳模式 Start of analysis with or . 激活“I”或“I/O”键开始分析。 Auto Zero Adjust and baseline determination of the IR detector for the TC peak. TC峰测定前,IR检测器基线的测定和自动零位的校正 Carrier gas will be turned off. 载气关闭。 Dosing of approx. 300 μl HCl into the reactor (syringe runs, valves switch). 将约300μl HCl注入反应器(注射器启动,阀门开关)。 Dosing of sample in the reactor (sampler runs, syringe runs, valves switch). 将样品注入反应器(进样器启动,注射器启动,阀门开关)。 Carrier gas will be turned on. 载气开启。 The temperature of the dynamic heater for the sample combustion increases up to max. 850°C. At the same time the integrator module waits for the TC measuring peak to start. 样品在动态加热器燃烧,温度升至850°C 。同时,积分器等待TC测量峰的开始。 TC peak integration. TC峰的积分 After exceding the peak maximum the dynamic heater will be turned off, the cooling fan works. 在超过峰的最大值之后,关闭动态加热器,冷却风扇开始工作。 Integration end 积分结束 Water drain 排水 Process end, a new start can be done. 程序结束,新的重新开始。 illustration 6.1: peak graphics TC determination 图示6.1:TC测定的峰图 NPOC Mode NPOC模式 Start of analysis with or . 激活“I”或“I/O”键开始分析。 Auto Zero Adjust and baseline determination of the IR detector for the TIC peak. TIC峰测定前,IR检测器基线的测定和自动零位的校正 Carrier gas will be turned off. 载气关闭。 Dosing of the sample in the reactor (sampler runs,syringe runs, valves switch). 将样品加入反应器(进样器启动,注射器启动,阀门开关)。 Dosing of the sample in the reactor (sampler runs, syringe runs, valves switch). 将样品注入反应器(进样器启动,注射器启动,阀门开关)。 Carrier gas will be turned on. 载气开启 At the same time the integrator module waits for the NPOC measuring peak to start. 同时,积分器等待NPOC测量峰的开始。 NPOC peak integration. NPOC峰的积分 Integration end 积分结束 Water drain 排水 Process end, a new start can be done. 程序结束,新的重新开始。 General notes to N

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