透射电子显微学课件解剖.ppt

M.S. Varela, et al., Phy. Rev. Lett. 92 (2004) 095502 STEM-EELS Atomic-Resolution Electron Energy Loss Spectroscopy La-doped CaTiO3 * 电子能量损失谱 张 庶 元 Electron Energy Loss Spectroscopy (EELS) 入射高能电子与样品的相互作用 * Atomic-scale view of electron energy loss in TEM Incident beam electron E0 (100 to 1000 keV) Excited specimen electron EB + E Scattered beam electron E0 - E K L Zero loss Electron energy loss (eV) Electrons count 0 1 eV 290 C K Inelastic scattering K L Elastic scattering Carbon atom What is an EELS spectrum? 电子能量损失谱信息 非弹性散射过程: 声子激发 (0.1eV) 等离子激发 (30eV) 内壳层电子激发