1 Professional Knowledge and Skills in Chemistry.pptVIP

* Characterization Notes Consider measuring the spectrum of a single fraction from a column, if purification is inefficient. If you have an OH or NH proton youd like to assign, add a drop of D2O to the sample, shake thoroughly, and take another proton spectrum. * Characterization Notes Often, enough information is gained from proton NMR spectroscopy to identify the product. Sometimes it is appropriate to gather more characterization data, and sometimes not. * Characterization Notes Continue with characterization when Your advisor recommends it. The compound is new and publication i