第10章综合分析举例(免费阅读).pptVIP

Fig 2. (c) Emission peak intensity of SWNT bound Fluor-PEG and free Fluor-PEG in a fluorescein concentration range of 200-900 nM. Figure 3. pH-dependent fluorescence and absorbance of Fluor-PEG/SWNT. Absorption curves of Fluor-PEG/SWNT at various pHs in the (a) fluorescein region (dashed line marks the peak at pH 12) . Figure 3. (b) SWNT region (curves are displaced for clarity). Figure 3. (c) Corresponding fluorescence emission spectra (ìexcitation ) 495 nm). Figure 3. (d) Comparison of emission peak intensity dependence on pH of free Fluor-PEG and Fluor-PEG/SWNT with the same Fluor-PEG concentration. Figure 4. Cellular uptake of Fluor-PEG/SWNT. (a) Confocal fluorescence image of BT474 cells incubated with Fluor-PEG/SWNT. Figure 4. (b) Fluorescence intensities of large population of cells treated with Fluor-PEG/SWNT vs untreated control cells by flow cytometry. Figure 4. (c) Micro-Raman image of the cells incubated with Fluor-PEG/SWNT. Figure 4. (d) Representative Raman spectra showing the presence and absence of the SWNT G-band from Fluor-PEG/ SWNT-incubated cells and untreated control cells, respectively. Preparation of polymer-coated mesoporous silica nanoparticles used for cellular imaging by a ‘‘graft-from’’ method 4 Yang Yang, Xuehai Yan, Yue Cui, Qiang He, Dongxiang Li,ac Anhe Wang, Jinbo Fei and Junbai Li etc J. Mater. Chem., 2008, 18, 5731–5737 | 5731 Fig. 1 SEM (A) and TEM (B, C) of MSN-NH2; TEM (D) of MSN@initiator. Fig. 2 XPS of MSN (a); MSN-NH2 (b); MSN@initiator (c) and MSN@polymer (M1) (d). Fig. 3 FTIR spectra of M1 (a); M2 (b); M3 (c) and MSN@initiator (d). Scheme 1 A schematic illustration of the surface functionalization for MSN and the fabrication of MSN@polymer. * 《材料研究方法》研究生课程 浙江工业大学 化工与材料学院 材料系 第10章 综合分析举例 Li-Ping Yang, Cai-Yuan Pan, Macromol. Chem. Phys. 2008, 209, 783-79