voc挥发性有机化合物分析方法.docVIP

泉岛公司色谱耗材专家 EPA 8260 Volatiles in Water Application 2432 GC/MS Technique : GC/MS Column : Fused Silica 60m x 0.32mm FactorFour VF-624ms, df=1.8 μm Part no.: CP9105 GC : CP3900 Temperature : 35 oC (2 min), 8 oC/min to 160 oC, 10 oC/min to 200 oC, 20 oC/min to 260 oC 5 min) Carrier gas : Helium, 1.2 mL/min Sampler : Tekmar 3000, purge and trap Injection : Split 1:20, Temp. 230 oC, 5 mL purge Detector : MS, Ion Trap 2100T; Temp. Trap: 150 oC, Temp. Manifold: 40 oC, Temp. Transfer line: 250 oC; Storage level of ms is set to exclude water and methanol ions Sample conc. : 10 ng / compo