工业分析以及马弗炉实用讲解.pptVIP

— 流化床及生物质能课题组 — — 流化床及生物质能课题组 — Vertical Electric Tube Furnace — 流化床及生物质能课题组 — — 流化床及生物质能课题组 — — 流化床及生物质能课题组 — — 流化床及生物质能课题组 — — 流化床及生物质能课题组 — — 流化床及生物质能课题组 — — 流化床及生物质能课题组 — — 流化床及生物质能课题组 — Thank you for your attention! * — 流化床及生物质能课题组 — The process and matters needing attention of biomass proximate analysis(生物质工业分析的过程及注意事项) Reporter: Hongmeng Hao Date: 2010.11.24 — 流化床及生物质能课题组 — Main points Test standard Matters needing attention The usage of the related apparatus — 流化床及生物质能课题组 — Test standard The received sample was cut, milled and sieved (对收到基进行切割、粉碎、筛分) External water content：drying oven 、55℃ (进行外水测量：烘箱、55℃) Wad=the lost mass/total mass×100 ，% (Wad=失水量/生物质重×100 ，%) every test was set one sample in parallel (在试验中每个生物质样设置两个平行样) Internal water content：1g、crucible、drying oven、105℃、3h、remove to a desiccator, cool to room temperature、weigh the residue (内水测量：1g、小方舟、烘箱、105℃、3h、干燥器内冷却至室温、称重) Wad=the lost mass/total mass×100 ，% (Wad=失水量/生物质重×100 ，% ) Test standard Ash centent:1g、 crucible 、muffle furnace、550℃、4h、400℃、drying in air for several minutes, remove to a desiccator, cool to room temperature、weigh the residue (灰分测量:1g、小方舟、马弗炉、550℃、4h、400℃、空气中冷却几分钟、放 入干燥器、冷却至室温、称重) Aad=the mass of residue/total mass×100 ，% (Aad=残渣物重量/生物质重×100 ，%) Test standard Volatile content：1g、crucible with cover、Vertical Electric Tube Furnace、900℃、7min、cool in air for five minutes、remove to a desiccator, cool to room temperature、weigh the residue (挥发分测量：1g、带盖坩埚、管式加热炉、900℃、7min、空气中冷却5分钟、放入干燥器中冷却至室温、称重) Vad=the lost mass/total mass×100-internal water content ，% (Vad=生物质加热减少重量/煤样重×100-水分 ，%) Test standard Fixed carbon：FCad=100-Mad-Aad-Vad (固定碳计算：FCad=100-Mad-Aad-Vad Test standard 1、internal water content testing Don’t plaster label onto the crucible （坩埚上不要用标签） 2、ash content testing 测灰分时 the heating rate of muffle furnace is round 5℃/min, until the muffle furnace rise to 550℃ from the room tempe