肿节风滴丸的质量标准研究.PDFVIP

中草药 Chinese Traditional and Herbal Drugs 41 8 2010 8 % 1303 % 刘根才, 戴德雄, 李金和* ( , 323000) : 99 10% , RSD 0 45% : ;; : R286 02 ; :B 1 3~ 9 7 g/ mL , : 0253 2670( 2010) 08 1303 02 , Sar candr a g labr a ( T hunb ) N akai ,, [ 1 2] , , [ 3] , 1 Agilent 1100 , ZB 1D , ZF 2 , BS124S , USC 502 ; ,, 2 21 , , : 1, 0 5% 5% , 1 m in, 0 3 g, 2, 2 0% , 22 : mL , 30 m in, 30 min, 25 m L, , 1, , 2 g, , ,5 50 mL , 2 , , 1 mL , , 0 5 m g/ m L , ( !2005 ? B) , 3 10 L, G , ( 9 # 4 # 1) , ,, , ( 365 nm) , ,; 10 min, 2 3 HPLC 2 31 : Diamonsil C18 ( 150 m m ? 4 6 mm, 5 m) ; : 0 1% ( 20 # 80) ; 1 mL / m in; 344 nm;