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Contact angle goniometry on single micron-scale fibers for composites.pdf

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Contact angle goniometry on single micron-scale fibers for composites.pdf

Applied Surface Science 392 (2017) 181–188 Contents lists available at ScienceDirect Applied Surface Science journal homepage: /locate/apsusc Contact angle goniometry on single micron-scale ?bers for composites Daniel Hansen a, Niels Bomholt b, Jonas Camillus Jeppesen a, Adam Cohen Simonsen a,? a Department of Physics Chemistry and Pharmacy, University of Southern Denmark, 5230 Odense M, Denmark b Covestro A/S, 5450 Otterup, Denmark article info Article history: Received 5 July 2016 Received in revised form 5 September 2016 Accepted 7 September 2016 Available online 13 September 2016 Keywords: Wetting Fibers Contact angle Composites Telecentric imaging abstract Probing the wetting properties of micro?bers by polymer resins is of signi?cant interest for the rational design of composite materials. Here, we demonstrate the measurement of contact angles on wetted micron scale ?bers by imaging the ?uid meniscus with telecentric optics at a spatial resolution of 4 ?m followed by automated image analysis. The meniscus is described as a catenary in the zero gravity approximation and by ?tting this to the measured pro?le, the contact angle is obtained at the intersection between the ?uid and the ?ber surface. The method is validated by measuring agreement between contact angles for the PMMA/H2O system for ?bers with diameters 20–800 ?m and for sessile drops. The ability of the method to discriminate contact angles for a series of commercial glass ?bers against epoxy resin is successfully demonstrated. AFM imaging shows that the surface topography of the ?bers does not have a simple relationship with the variation in contact angles. Contact angle goniometry by imaging of micron scale ?bers appears as a viable alternative to Wilhelmy type measurements and the measurement principle could readily be extended to dynamic wetting experiments. ? 2016 Elsevier B.V. All rights reserved. 1. Introduction Composite materials are widely used in a variety of ?elds for the construction of s