SolvothermalSynthesisandMicrowaveAbsorbingPropertiesof.pdfVIP

Material Sciences 材料科学, 2011, 1, 65-70 /10.12677/ms.2011.12013 Published Online July 2011 (/journal/ms/) Solvothermal Synthesis and Microwave Absorbing Properties of Fe O Microspheres and MWCNT/Fe O 3 4 3 4 Heterostructures * Changfa Guo, Qingmei Su, Gaohui Du, Yong Hu Zhejiang Key Laboratory for Reactive Chemistry on Solid Surfaces and Institute of Physical Chemistry, Zhejiang Normal University, Jinhua Email: yonghu@; changfag@ Received: Mar. 29th, 2011; revised: Jun. 5th, 2011; accepted: Jun. 7th, 2011. Abstract: Fe O microspheres were prepared via a facile solvothermal method using hydrous ferric chloride and 3 4 anhydrous sodium acetate as materials, and ethylene glycol as solvent. Furthermore, the tunable denseness car- bon nanotubes (MWCNTs)/Fe O heterostructures were obtained by adjusting the ratio of ferric chloride and 3 4 MWCNTs in the reaction system. The morphology and phase of the products were characterized by scanning electron microscope (SEM) and X-ray diffractometer (XRD). The results show that Fe O microspheres with hi- 3 4 erarchical structure wrap discontinuously on MWCNTs in the hybrids, and wrapping density increase with re- duction of the amount of MWCNTs. The Fe O microspheres with an unchanged phase in the heterostructures 3 4 are composed of sma