甘遂提取物(国外英文资料).docVIP

甘遂提取物 [product name] gan sui extract [English name] Kansui Root P.E. 【 abstract 】 the dry root of Euphorbia kansui Liou. MSS. When the spring blossoms or the late autumn leaves wilt, they will be dug up, and they will run into the skin and dry. 】 【 chemical composition containing alpha and gamma spurge sterol (alpha and gamma - euphorbol), euphorbia kansui sterol (tirucallol), and contains 13 - oxidation huge ji terpene alcohols (13 - oxyingenol), euphorbia kansui terpene ester of A and B (kansuinineA, B), etc. [product spec] 10:1 TLC 【 color 】 brown and yellow fine powder [physical and chemical identification] 1. Take the powder of the ethanol solution and reference substance spurge sterol sample points respectively in silica G thin layer plate, with benzene - ethanol (4:1)/n-heptane - benzene (1:1), acetic anhydride, sulfuric acid injection (1:1) color, the sample and reference substance in the corresponding position show the same color of the purple spots. Take the powder 10g, add 80% ethanol, 100ml, chill for 7 days, shake it three times a day, filter it. Take 50ml of filtrate, remove ethanol from water bath, and use benzene to extract 4 times, each time 10ml, merge to 50ml, as a sample solution. Another sample powder 10 g, 100 ml of water, airtight, 4 hours at 90 ° C insulation filtration. Take 50ml plus ethanol 200ml, place overnight, filter, residue with 75% ethanol wash, filtrate in water bath, remove ethanol, and use benzene to extract as a sample solution. Take the above two types of sample liquid and apply it to the silicone G lamella, which is carried out with the oil ether - acetate (90:3), with the sulfur vapor and the flecks of yellow. The number of products is 100 percent through 80 mesh 【 functional 】 The abdomen is full of edema. With the two money, two and a half, the total grind is the end of the whole, fry as a water agent, take at any time. A bloated body. In the case of the pig kidney, the wet paper is cooked and cooked. Eat once to four or f