油田用乳化剂乳化力的测定方法改进.pdfVIP

学兔兔 化 工 进 展 CHEMICAL INDUSTRY AND ENGINEERING PROGRESS 2012年第3 l卷第8期 油田用乳化剂乳化力的测定方法改进 张 翼 ，王德虎 ，林庆霞 ，朱友益 ，龙 杭 ( 中国石油勘探开发研究院采收率所，北京 100083； 中国地质大学能源学院，北京 100083) 摘 要：为了使油田用助剂的乳化力的评定与实际工作环境更为吻合，实验改进了原有的国家标准，采用光度 法进行了实验研究 确立了分析方法的最佳波长为230nln附近，标准曲线绘制时的油含量选在300mg／L以下时 线性关系良好，乳化剂的用量在0．05％(质量分数)以上时具有较好的乳化现象，便于操作。给出了操作步骤和 溶液配制规程，验证了该方法的误差、重现性和实用性，表明该法可以有效地评定油田用表面活性剂的乳化力。 关键词：油田；乳化剂；乳化力；测定方法 中图分类号：TE 39 文献标志码：A 文章编号：1000—6613(2012)08—1852—05 The emulsifying ability determination of an emulsifier used in oil field ZHANG Yi ，WANG Dehu ，LINQingxia ，ZHUYouyi ，LONG Hang (1Enhanced Oil Recovery Department，Research Institute ofPetroleum Exploration and Development，CNPC，Beijing 100083，China~ School ofEnergyResources，ChinaUniversity ofGeosciences，Beijing 100083，China) Abstraet-In order to determine the emulsi ing ability of an emulsifier used in oil field more consistently with the actual WOrking environment，this experiment result can improve the current national standards．For spectrophotometry method，the best wavelength is 230nm．The oil content for the standard curves should be controlled less than 300mg／L．The dosage of emulsifier should be more than 0．O5％．The operation procedure of determination process and me solution preparation method were setup．The error，reproducibility and practicality of the method were veilfled．The results indicate that the method is an effective for evaluating the emulsifling ability of surfactants used in oil field． Key words：oil field；emulsifier；emulsifl，ing ability：determination method 随着国内陆相油田开发的深入，提高原油采收 的【4