钛酸铵 介稳层状相.pdfVIP

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钛酸铵 介稳层状相.pdf

Spiky mesoporous anatase titania beads… … have been fabricated and are described in the Full Paper by R. A. Caruso et al. on page 13762 ff. These unique nanostructures were prepared through a controllable phase transformation and crystalliza- tion process from amorphous precursor beads to metastable amorphous titania/ammonium titanate core-shell structures, and then finally to anatase beads. The resultant spiky titania beads show great po- tential as working electrodes for high-performance dye-sensitized solar cells. DOI: 10.1002/chem.201202539 Spiky Mesoporous Anatase Titania Beads: A Metastable Ammonium Titanate-Mediated Synthesis Dehong Chen,[a] Fuzhi Huang,[b] Lu Cao,[a] Yi-Bing Cheng,*[b] and Rachel A. Caruso*[a, c] Abstract: A complex titania nanostruc- revealed by HRTEM characterization, tanate intermediate, on further heating ture of monodisperse spiky mesopo- are single crystals elongated along the the final spiky mesoporous titania rous anatase beads composed of ana- c axis of the tetragonal anatase titania. beads were clearly observed. This tita- tase nanocrystals with diameters of less The resultant spiky titania beads have nate-phase-mediated approach allows than 15 nm in the core and much larger high surface areas of up to 112 m2g1 control over the size of the nanocrys- hollow-cone shaped spikes on the sur- and pore diameters and pore volumes tals in the core of the bead, as well as face was fabricated using a facile solvo- that vary depending on the ammonia the anatase spikes on the surface, and thermal process in the presence of am- concentration and solvothermal treat-

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