实验室中注意点（Notice in the lab）.docVIP

实验室中注意点（Notice in the lab） When doing high-pressure reaction experiment, must not be able to carry pressure operation! Be sure to check if the air tube is open when moving the valve and screw. Otherwise, it may fly. It is very dangerous! Everyone doing the experiment carefully, not paralysis, vacuum distillation, once I do not put the condensing system fixed in mind, the results oh, solvent jetted out from the bottle, SOB, products are sprayed out! Worked in hydrogen storage test of LaNi5 powder dont pour directly to the trash can, because of very fine particles easy oxidation burning, our lab I have seen a few times, well someone, or consequences, had better use a wet paper bag. When you need to control the PH, you have to use the acid meter, dont use the test paper, I did an experiment, the two are three minus four, haha, you can imagine The format reaction requires no water tetrahydrofuran, which USES sodium metal to remove water. After steaming, the flask was placed for a few days, mistakenly believing that the sodium had been fully reacted, without adding alcohol and adding water directly to it, and there was no abnormality in the beginning. After a while, it began to smoke... Blast! Fortunately only minor injuries. What a shock! Sodium peroxide reacts with water to be tested with a Mars bar. Because of the ordinary individual chemical experiment accomplishment not how. All are greedy! I took three tablespoons of sodium peroxide, but only added a few drops of water, and tested it with a Mars bar. Later curious about the new heart action, I took the Mars stick to the bottom of the test tube, the result -- explosion! Fortunately, I took the test tube in a hard tube. Otherwise the small life is gone! The reason: there is a lot of sodium peroxide and a small amount of oxygen at the bottom of the tube. Take the Mars bar to the bottom of the test tube, first produce the carbon dioxide, and the carbon dioxide reacts with the sodium peroxide to produce oxygen, and then