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6卷(6 rolls)
6卷(6 rolls)
Fill in the blanks. (1 points per minute, 20 points altogether)
1 distillation is one of the most commonly used methods of separation and purification. This method can not only separate () from (), but also separate substances with different boiling points and colored impurities.
2) is a distillation that can be accomplished at a time by means of a fractionating column that does not require repeated repetitions of a series of distillation.
3, the extraction of emulsification phenomenon, according to the actual situation, using (), (), () and other methods of demulsification.
4, when the toxic and irritating gas produced in the reaction, use the gas absorption device to absorb harmful gases. The choice of absorbent depends on () determination. For example, hydrogen halides can be absorbed by (or); absorbed chlorine and other acidic gases.
5. Aniline is a common reagent in organic chemical reactions. In our experiments, reactions involving aniline (including) and ().
6, according to the chromatographic separation principle can be divided into (), (), () and steric exclusion chromatography; according to the different operating conditions can be divided into (), (), (), gas chromatography and high performance liquid chromatography.
7, heat filtration can remove insoluble impurities, decoloring agents and other impurities. Include (), () two methods.
Two, multiple-choice questions. (2 points per game, 20 points)
1. Because most adsorbents are strongly absorbent, they usually bake for 30 minutes under () conditions.
A, 100 B and 105 DEG C
C, 110 D and 115 DEG C
2. The role of chromatography in organic chemistry mainly includes ().
A, isolation and purification of B and identification of compounds
C, determination of compound purity, monitoring of D and organic reactions
3, in the post treatment process of acetylsalicylic acid, we adopted () to purify the product.
A, recrystallization, B, acidification, alkalization, C, alkalization and acidification
4, in orde
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