分析化学实验（Analytical chemistry experiment）.docVIP

分析化学实验（Analytical chemistry experiment） One Analytical chemistry experiment; quantitative analysis; thinking question; answer Quantitative analysis experiment Experiment 1. Weighing exercises in weighing exercises. 1.. When adding weights, weights, loops, weights and weights, why must we close the scales? Answer: the sensitivity of the balance depends to a great extent on the quality of the three agate edges. If the knife edge is not sharp or defective, it will affect the sensitivity of weighing; therefore, when the weights are added and removed, the scales must be closed so that the agate knife and the knife support are separated, so as to protect the agate blade. 2., the higher the sensitivity of the balance, whether the accuracy of weighing is higher? Answer: the higher the sensitivity of an analytical balance, the higher the accuracy of the weighing. Because it is too sensitive, it is difficult to achieve balance and is not easy to weigh. 3.. Can you use a spoon to sample in the weighing process? Why? Answer: descending weighing method, weighing process can not use small spoon sampling, because weighing parts have to be dipped in small spoon, affect weighing accuracy. 4. in the weighing process, observed the marking has been moved to 100 degrees right from the projection screen, the left or right heavy weight? A: in the weighing process, the reticle has been moved to the right of the 100 division from the projection screen, indicating that the right disk is heavy. Experiment two. Basic exercises of titration analysis. Thinking questions: can 1.HCl and NaOH standard solution be prepared by direct compounding? Why? Answer: because the NaOH solid absorbs CO2 and moisture in the air, the concentration of concentrated HCl is uncertain, and HCl and NaOH standard solutions can not be prepared by direct method. 2. preparation of acid standard solution, why measure out HCl, with scales that take NaOH (S), instead of the pipette and analytical balance? Answer: because the