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zyhx_jy0301(zyhx _ jy0301)
zyhx_jy0301(zyhx _ jy0301)
Three, spectrum
(a) ultraviolet spectrum (UV)
1. flavonoids
The UV spectrum of flavonoids in methanol solution can be used to distinguish between different types of flavonoids:
Flavonoids, flavonols, chalcones have I, II, but flavonoids, flavonol with I absorption intensity in zone II, but chalcone with I absorption intensity is weaker than the band II, two opposite. Flavone, flavonol by with the maximum absorption wavelength of I is identified, less than 350nm is greater than 350nm and flavonoids, flavonols.
Isoflavone, two hydrogen Huang Tong (alcohol) are only 2, without I, methanol only showed 1 peaks of spectra. The isoflavone band II maximum absorption peak wavelength is less than or equal to 270nm, two hydrogen Huang Tong (alcohol) is greater than 270nm, identification. While the two hydrogen flavonoids and two flavanonols because there is no I, not identified by UV, only with the help of hydrogen spectrum.
B type questions
A. flavonoids
B.5- dihydroxyflavone
C.5,6,7- three hydroxyflavone
D. flavanone
E.5- hydroxy flavanone
The 1. peaks in the UV band II absorption around 262nm (is)
Answer [No. 981030101]
Answer [B]
The 2. peaks in the UV band II absorption around 274nm (is)
Answer [No. 981030102]
Answer [C]
The 3. peaks in the UV band II absorption around 250nm (is)
Answer [No. 981030103]
Answer [A]
2. cardiac glycoside
The maximum absorption wavelength of cardenolide UV is 217 ~ 220nm, the maximum absorption wavelength of ultraviolet B cardiac glycosides was 295 ~ 300nm,
A type questions:
UV features of cardiac aglycone 1. B absorption wavelength range is ()
A.215 ~ 220nm
B.225 ~ 240nm
C.250 ~ 270nm
D.265 ~ 285nm
E.295 ~ 300nm
Answer [No. 981030104]
Answer [E]
The maximum absorption of ultraviolet B 2. cardiac glycosides (is)
A.217 ~ 220nm
B.295 ~ 300nm
C.345 ~ 350nm
D.350 ~ 360nm
E.370 ~ 400nm
Answer [No. 981030105]
Answer [B]
B type questions
A.217 ~ 220nm
B.270 ~ 278nm
C.295 ~ 300nm
D.300 ~ 330nm
E.217 ~ 220nm, 270nm
1. element
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